Structures published

Total: 358

Dimethyl 3-acetyl-3-(1,3-benzothiazol-2-yl)pentanedioate

C₁₆H₁₇NO₅S

Baryala, Yamna Salem, Moussa Essassi, El Mokhtar Reuter, Hans Izaaryene, Maher

Acta Crystallographica Section E (2008) 64, 12 o2290

a=14.4075(3)Å b=8.8089(2)Å c=13.8968(3)Å

α=90.00° β=118.0110(10)° γ=90.00°

6-Methyl-7,7,9-tripropargyl-7H-1,2,4- triazolo[4,3-b][1,2,4]triazepin-8(9H)-one

C₁₅H₁₃N₅O

Zemama, Redwan Mohamed Amari, Ibtissam Bouhfid, Rachid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 9 o2148

a=7.6710(2)Å b=8.2415(2)Å c=12.9619(3)Å

α=108.5100(10)° β=90.6590(10)° γ=114.7260(10)°

1-Benzyl-3-[(dimethylamino)methylene]-4-phenyl-1H- 1,4-benzodiazepin-2(3H)-one

C₂₅H₂₃N₃O

Zemama, Redwan Mohamed Amari, Ibtissam Bouhfid, Rachid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 9 o2160

a=8.9733(3)Å b=26.3103(7)Å c=9.9312(3)Å

α=90° β=115.6440(10)° γ=90°

7,9-Diallyl-6-methyl-7H-1,2,4-triazolo[4,3-b][1,2,4]triazepin-\ 8(9H)-one

C₁₂H₁₅N₅O

Zemama, Redwan Mohamed Amari, Ibtissam Bouhfid, Rachid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 9 o2152

a=7.4674(3)Å b=8.3398(3)Å c=20.2214(6)Å

α=90.00° β=95.174(2)° γ=90.00°

3-Methyl-1-propargylquinoxalin-2(1H)-one

C₁₂H₁₀N₂O

Benzeid, Hanane Ramli, Youssef Vendier, Laure Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 9 o2196

a=21.1240(10)Å b=4.3709(2)Å c=22.2460(10)Å

α=90.00° β=105.354(6)° γ=90.00°

5-Methyl-3-[1-(2-pyridylmethyl)-1H-benzimidazol-2-ylmethyl]isoxazole

C₁₈H₁₆N₄O

Doumbia, Mohamadou Lamine Bouhfid, Rachid Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2009) 65, 11 o2714-o2715

a=11.0761(2)Å b=8.65350(10)Å c=16.5920(3)Å

α=90.0° β=103.1360(10)° γ=90.0°

3-[2-(3-Methyl-2-oxo-1,2-dihydroquinoxalin-1-yl)ethyl]oxazolidin-2-one

C₁₄H₁₅N₃O₃

Caleb, Ahoya Anothane Bouhfid, Rachid Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2009) 65, 8 o2024-o2025

a=12.280(3)Å b=10.736(3)Å c=20.406(4)Å

α=90° β=102.320(10)° γ=90°

1-Allyl-4-phenyl-2,3-dihydro-1H-1,5-benzodiazepin-2-one

C₁₈H₁₆N₂O

Ballo, Daouda Ahabchane, Noureddine Hamou Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1277

a=11.4863(3)Å b=6.0053(2)Å c=20.3667(5)Å

α=90.00° β=93.5250(10)° γ=90.00°

1-(1-Nonyl-2-oxoindolin-3-ylidene)thiosemicarbazide

C₁₈H₂₆N₄OS

Mamari, Khalil Zerzouf, Abdelfettah Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1332

a=11.5343(2)Å b=10.5921(2)Å c=15.6262(3)Å

α=90.00° β=95.9220(10)° γ=90.00°

1-(1-Decyl-2-oxoindolin-3-ylidene)thiosemicarbazide

C₁₉H₂₈N₄OS

Mamari, Khalil Zerzouf, Abdelfettah Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1333

a=11.8856(2)Å b=11.0055(2)Å c=15.1638(3)Å

α=90.00° β=99.4680(10)° γ=90.00°

1-Tetradecylindoline-2,3-dione

C₂₂H₃₃NO₂

Mamari, Khalil Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1410

a=27.6647(8)Å b=4.70550(10)Å c=15.7583(5)Å

α=90.00° β=103.6350(10)° γ=90.00°

1-Decylindoline-2,3-dione

C₁₈H₂₅NO₂

Mamari, Khalil Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1411

a=22.7208(3)Å b=4.71890(10)Å c=15.82540(10)Å

α=90.00° β=106.8270(10)° γ=90.00°

Ethyl {4-[(1,5-dimethyl-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5- benzodiazepin-3-yl)methyl]-1,2,3-triazol-1-yl}acetate

C₁₈H₂₁N₅O₄

Dardouri, Rachida Kandri Rodi, Youssef Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 11 o3039

a=8.5452(2)Å b=15.9993(5)Å c=13.9215(4)Å

α=90.00° β=106.8530(10)° γ=90.00°

3-[(1-Benzyl-1H-1,2,3-triazol-5-yl)methyl]-6-bromo-2-phenyl- 3H-imidazo[4,5-b]pyridine

C₂₂H₁₇BrN₆

Ouzidan, Younes Kandri Rodi, Youssef Fronczek, Frank R.Venkatraman, Ramaiyer Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 4 o890-o891

a=41.122(6)Å b=5.8358(10)Å c=15.988(3)Å

α=90° β=93.922(6)° γ=90°

Methyl 2-(3-oxo-3,4-dihydro-2H-1,4-benzothiazin-4-yl)acetate

C₁₁H₁₁NO₃S

Barryala, Yamna Massip, Stéphane Lazar, Saïd Essassi, El Mokhtar Zouihri, Hafid

Acta Crystallographica Section E (2011) 67, 3 o724

a=17.347(5)Å b=8.724(2)Å c=7.2740(10)Å

α=90.00° β=98.71(2)° γ=90.00°

1,3-Dimethyl-3-tetradecyl-1H-1,5-benzodiazepine- 2,4(3H,5H)-dione

C₂₅H₄₀N₂O₂

Dardouri, Rachid Ouazzani Chahdi, Fouad Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 3 o674

a=8.12860(10)Å b=33.5899(5)Å c=9.4095(2)Å

α=90.00° β=114.6400(10)° γ=90.00°

3-{[3-(4-Chlorophenyl)-4,5-dihydro-1,2-oxazol-5-yl]methyl}-1,5-dimethyl- 1H-1,5-benzodiazepine-2,4(3H,5H)-dione

C₂₁H₂₀ClN₃O₃

Dardouri, Rachida Rodi, Youssef Kandri Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 3 o720

a=8.18210(10)Å b=9.07410(10)Å c=13.3792(2)Å

α=79.7480(10)° β=80.1420(10)° γ=85.9100(10)°

5-Nitro-1-nonyl-1H-benzimidazol-2(3H)-one

C₁₆H₂₃N₃O₃

Ouzidan, Younes Kandri Rodi, Youssef Essassi, El Mokhtar El Ammari, Lahcen Fronczek, Frank R.Venkatraman, Ramaiyer

Acta Crystallographica Section E (2011) 67, 3 o669

a=5.4830(10)Å b=10.2092(15)Å c=14.746(3)Å

α=74.275(9)° β=79.727(6)° γ=83.410(8)°

3-[2-(3-Methylquinoxalin-2-yloxy)ethyl]-1,3-oxazolidin-2-one

C₁₄H₁₅N₃O₃

Ahoya, Caleb Anothane Bouhfid, Rachid Daouda, Ballo Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2010) 66, 5 o1050

a=6.9936(3)Å b=7.6916(3)Å c=13.3709(6)Å

α=86.649(2)° β=77.044(2)° γ=71.141(2)°

(E)-4-(2,3-Dihydro-1,3-benzothiazol-2-ylidene)-3-methyl-1-phenyl- 1H-pyrazol-5(4H)-one

C₁₇H₁₃N₃OS

Chakibe, Imane Zerzouf, Abdelfettah Essassi, El Mokhtar Reichelt, Martin Reuter, Hans

Acta Crystallographica Section E (2010) 66, 5 o1096

a=27.0144(8)Å b=7.4021(2)Å c=14.0523(4)Å

α=90.00° β=97.4660(10)° γ=90.00°

3-Methyl-1-(prop-2-en-1-yl)quinoxalin-2(1H)-one

C₁₂H₁₂N₂O

Ramli, Youssef Slimani, Rachid Zouihri, Hafid Lazar, Saïd Essassi, E. M.

Acta Crystallographica Section E (2010) 66, 7 o1767

a=5.0722(5)Å b=13.4707(13)Å c=15.0507(13)Å

α=90.00° β=95.082(5)° γ=90.00°

3-[2-(5H-Indolo[2,3-b]quinoxalin-5-yl)ethyl]-1,3-oxazolidin-2-one

C₁₉H₁₆N₄O₂

Alsubari, Abdussalam Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 9 o2461

a=14.5565(4)Å b=5.8993(2)Å c=18.6434(6)Å

α=90.00° β=92.393(2)° γ=90.00°

1-Nonyl-1H-benzimidazol-2(3H)-one

C₁₆H₂₄N₂O

Ouzidan, Younes Kandri Rodi, Youssef Butcher, Raymond J.Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 2 o283

a=18.0230(10)Å b=5.4585(2)Å c=16.5708(9)Å

α=90.00° β=115.543(7)° γ=90.00°

1,3-Bis[2-(2-oxo-1,3-oxazolidin-3-yl)ethyl]-1H-benzimidazol- 2(3H)-one

C₁₇H₂₀N₄O₅

Ouzidan, Younes Kandri Rodi, Youssef Fronczek, Frank R.Venkatraman, Ramaiyer El Ammari, Lahcen Essassi, El Mokhtar

Acta Crystallographica Section E (2011) 67, 2 o362-o363

a=10.5331(10)Å b=10.9647(10)Å c=14.5541(14)Å

α=90° β=103.258(5)° γ=90°

4-Phenyl-9,12,15-trioxa-1,5,6,18- tetraazatetracyclo[16.6.1.0^2,6^.0^19,24^]pentaconta-2,4,19,21,23- pentaen-25-one

C₂₄H₂₆N₄O₄

Ghomsi, Joseph Nathan Ahabchane, Noureddine Hamou Bouhfid, Rachid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 10 o2493

a=13.3480(10)Å b=15.7850(10)Å c=11.0070(10)Å

α=90° β=102.6810(10)° γ=90°

1,3-Diallyl-2-methylbenzimidazolium bromide dihydrate

C₁₄H₁₇N_2,Br_,2H₂O

Ennajih, Hamid Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 10 o2321

a=13.2888(2)Å b=16.8763(2)Å c=7.38970(10)Å

α=90.00° β=109.7730(10)° γ=90.00°

\ 10-Allyl-2,3-dihydro-1H-pyrrolo[2,1-c][1,4]benzodiazepine-5,\ 11(10H,11aH)-dione

C₁₅H₁₆N₂O₂

Benzeid, Hanane Essassi, El Mokhtar Saffon, Nathalie Garrigues, Bernard Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 10 o2322

a=7.09880(10)Å b=11.7166(2)Å c=15.6592(3)Å

α=90.00° β=90.00° γ=90.00°

1-Methyl-3-phenylquinoxalin-2(1H)-one

C₁₅H₁₂N₂O

Benzeid, Hanane Essassi, El Mokhtar Saffon, Nathalie Garrigues, Bernard Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 10 o2323

a=16.3919(5)Å b=7.0775(2)Å c=20.0214(6)Å

α=90.00° β=95.434(2)° γ=90.00°

1-Allyl-3-chloro-6-nitro-1H-indazole

C₁₀H₈ClN₃O₂

El Brahmi, Nabil Mohamed, Benchidmi Essassi, El Mokhtar Zouihri, Hafid Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 10 o2320

a=7.68040(10)Å b=9.9559(2)Å c=28.4344(4)Å

α=90° β=95.1440(10)° γ=90°

1-Benzyl-3-phenylquinoxalin-2(1H)-one

C₂₁H₁₆N₂O

Benzeid, Hanane Saffon, Nathalie Garrigues, Bernard Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 11 o2685

a=5.4776(2)Å b=12.7015(3)Å c=12.7469(4)Å

α=62.260(2)° β=89.963(2)° γ=87.845(2)°

10,10'-Methylenebis[2,3-dihydro-1H- benzo[e]pyrrolo[1,2-a][1,4]diazepine- 5,11(10H,11aH)-dione] dihydrate

C₂₅H₂₄N₄O_4,2(H₂O)

Benzeid, Hanane Saffon, Nathalie Garrigues, Bernard Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 11 o2684

a=11.9901(2)Å b=11.9901Å c=13.6054(2)Å

α=90° β=90° γ=120°

1-Acetyl-4-phenyl-5a,6,7,8,9,9a-hexahydro-5H- 1,5-benzodiazepin-2(1H)-one

C₁₇H₂₀N₂O₂

Benzeid, Hanane Saffon, Nathalie Garrigues, Bernard Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2009) 65, 11 o2657

a=9.6794(2)Å b=14.0095(3)Å c=11.2832(2)Å

α=90° β=98.0530(10)° γ=90°

4-[(1,5-Dibenzyl-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin- 3-yl)methyl]-1-n-octyl-1H-1,2,3-triazole

C₃₄H₃₉N₅O₂

Jabli, Hind Ouazzani Chahdi, F.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 1 o231

a=9.1797(2)Å b=10.4238(2)Å c=31.4716(7)Å

α=90.00° β=90.00° γ=90.00°

1-(12-Azido-n-dodecyl)-4-[(1,5-dibenzyl-2,4-dioxo-2,3,4,5-tetrahydro-\ 1H-1,5-benzodiazepin-3-yl)methyl]-1H-1,2,3-triazole

C₃₈H₄₆N₈O₂

Jabli, Hind Ouazzani Chahdi, F.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 1 o232

a=9.4269(2)Å b=12.3304(3)Å c=15.5500(4)Å

α=101.121(2)° β=92.175(2)° γ=92.935(2)°

Ethyl 2-{4-[(1,5-dibenzyl-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5- benzodiazepin-3-yl)methyl]-1H-1,2,3-triazol-1-yl}acetate

C₃₀H₂₉N₅O₄

Jabli, Hind Kandri Rodi, Y.Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 1 o126

a=14.2015(5)Å b=10.9337(4)Å c=17.9368(6)Å

α=90.00° β=95.699(2)° γ=90.00°

3-[2-(2,3-dioxoindolin-1-yl)ethyl]-1,3-oxazolidin-2-one

C₁₃H₁₂N₂O₄

Al Subari, Abdusalam Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 2 o454

a=7.1198(2)Å b=7.4694(2)Å c=12.0319(3)Å

α=83.338(2)° β=79.084(2)° γ=81.372(2)°

1,3-Dibenzyl-2-methylbenzimidazolium chloride

C₂₂H₂₁N_2,Cl

Ennajih, Hamid Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 2 o455

a=9.2539(2)Å b=9.4677(2)Å c=12.0984(3)Å

α=72.1390(10)° β=81.3760(10)° γ=64.6050(10)°

6-Bromo-1-[2-(2-oxo-1,3-oxazolidin-3-yl)ethyl]-1H- imidazo[4,5-b]pyridin-2(3H)-one

C₁₁H₁₁BrN₄O₃

Bel-Ghacham, H.Kandri Rodi, Y.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 2 o456

a=27.0174(11)Å b=6.0141(2)Å c=16.6121(6)Å

α=90.00° β=110.343(2)° γ=90.00°

3-(Phenylimino)indolin-2-one

C₁₄H₁₀N₂O

Al Subari, Abdusalam Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 2 o453

a=20.1647(4)Å b=5.02230(10)Å c=21.8791(5)Å

α=90.00° β=90.00° γ=90.00°

3-[(1-Benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,5-dimethyl- 1,5-benzodiazepine-2,4-dione

C₂₁H₂₁N₅O₂

Dardouri, R.Kandri Rodi, Y.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 3 o632

a=8.3380(3)Å b=9.1033(3)Å c=13.4796(4)Å

α=95.385(2)° β=107.840(2)° γ=101.768(2)°

3-[(1-Benzyl-1H-1,2,3-triazol-5-yl)methyl]-1,5-dimethyl- 1,5-benzodiazepine-2,4-dione monohydrate

C₂₁H₂₁N₅O_2,H₂O

Dardouri, R.Kandri Rodi, Y.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 3 o633

a=9.60020(10)Å b=11.9497(2)Å c=17.0860(2)Å

α=90.00° β=92.5270(10)° γ=90.00°

2-Hydroxy-10-propargylpyrrolo[2,1-c][1,4]benzodiazepine-5,11-dione monohydrate

C₁₅H₁₄N₂O_3,H₂O

Ourahou, S.Chammache, M.Zouihri, H.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o731

a=6.89770(10)Å b=7.97610(10)Å c=13.0680(2)Å

α=90.00° β=99.1940(10)° γ=90.00°

2-Hydroxy-10-phenacylpyrrolo[2,1-c][1,4]benzodiazepine-5,11-dione

C₂₀H₁₈N₂O₄

Ourahou, S.Chammache, M.Zouihri, H.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o732

a=8.8337(2)Å b=9.9476(2)Å c=18.9295(4)Å

α=90.00° β=90.00° γ=90.00°

Ethyl 2-hydroxy-5,11-dioxopyrrolo[2,1-c][1,4]benzodiazepine-10-acetate

C₁₆H₁₈N₂O₅

Ourahou, S.Chammache, M.Zouihri, H.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o733

a=8.5503(2)Å b=9.6580(2)Å c=18.2734(4)Å

α=90.00° β=90.00° γ=90.00°

2-Methyl-3-(n-octylsulfanyl)quinoxaline

C₁₇H₂₄N₂S

Ramli, Youssef Slimani, Rachid Zouihri, Hafid Lazar, Saïd Essassi, E. M.

Acta Crystallographica Section E (2010) 66, 4 o992

a=7.3514(3)Å b=8.2978(3)Å c=14.2168(5)Å

α=92.275(2)° β=98.706(2)° γ=103.810(2)°

N-(5-Phenyl-1H-pyrazol-3-yl)benzene-1,2-diamine

C₁₅H₁₄N₄

Doumbia, Mohamadou Lamine Bouhfid, Rachid Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2010) 66, 4 o841

a=13.2357(8)Å b=5.8473(4)Å c=16.4039(10)Å

α=90.00° β=92.074(4)° γ=90.00°

6-Bromo-1-(1,2-propadienyl)-3-(2-propynyl)-1H- imidazo[4,5-b]pyridin-2(3H)-one

C₁₂H₈BrN₃O

Dahmani, S.Haoudi, A.Capet, F.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o755

a=9.6369(4)Å b=9.3086(4)Å c=13.5481(5)Å

α=90.00° β=99.123(2)° γ=90.00°

6-Bromo-1,3-di-2-propynyl-1H-imidazo[4,5-b]pyridin- 2(3H)-one

C₁₂H₈BrN₃O

Dahmani, S.Haoudi, A.Capet, F.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o756

a=9.0725(3)Å b=18.6212(5)Å c=7.0684(2)Å

α=90.00° β=102.9950(10)° γ=90.00°

3-(Benzothiazol-2-yl)-3-(prop-2-ynyl)hex-5-yn-2-one

C₁₆H₁₃NOS

Baryala, Yamna Zerzouf, Abdelfettah Salem, Moussa Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2010) 66, 4 o857

a=7.79130(10)Å b=30.2051(6)Å c=12.4437(2)Å

α=90.00° β=106.1610(10)° γ=90.00°

4-Benzyl-6-bromo-2-phenyl-4H-imidazo[4,5-b]pyridine

C₁₉H₁₄BrN₃

Ouzidan, Y.Obbade, S.Capet, F.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o946

a=8.6613(6)Å b=19.7631(13)Å c=9.3683(6)Å

α=90.00° β=99.647(3)° γ=90.00°

4-Benzyl-6-bromo-2-(4-methoxyphenyl)-4H-imidazo[4,5-b]pyridine monohydrate

C₂₀H₁₆BrN₃O_,H₂O

Ouzidan, Y.Kandri Rodi, Y.Obbade, S.Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 4 o947

a=10.5924(2)Å b=5.45440(10)Å c=31.7444(7)Å

α=90.00° β=100.2920(10)° γ=90.00°

6-Bromo-3-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

C₇H₆BrN₃O

Ghacham, Hend Bel Rodi, Youssef Kandri Capet, Frédéric Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 5 o1080

a=4.41510(10)Å b=9.6004(2)Å c=10.5330(3)Å

α=116.2480(10)° β=93.074(2)° γ=91.6870(10)°

1-Benzyl-3-[(dimethylamino)methylene]-4-phenyl-1H-1,5-benzodiazepine- 2(3H)-thione

C₂₅H₂₃N₃S

Ballo, Daouda Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 5 o1019

a=26.4740(8)Å b=10.2366(2)Å c=16.5650(5)Å

α=90.00° β=106.1360(10)° γ=90.00°

8-Bromo-3,4-dihydro-2H1,3-thiazino[2,3:2',1']imidazo[5',4'- b]pyridine

C₉H₈BrN₃S

Ghacham, Hend Bel Rodi, Youssef Kandri Capet, Frédéric Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 5 o1079

a=20.2738(3)Å b=13.2786(2)Å c=7.31690(10)Å

α=90.00° β=102.1930(10)° γ=90.00°

3,4-Dimethyl-1H-1,2,4-triazepino[2,3-a]benzimidazol- 2(3H)-one

C₁₂H₁₂N₄O

Saber, Asmae Al Subari, Abdusalam Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 5 o1093

a=7.2899(3)Å b=14.4888(5)Å c=10.9932(4)Å

α=90.00° β=104.3140(10)° γ=90.00°

1-Isopropenyl-1H-1,3-benzimidazol-2(3H)-one

C₁₀H₁₀N₂O

Saber, Asmaa Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1409

a=15.8724(2)Å b=6.09710(10)Å c=17.9313(3)Å

α=90.00° β=90.961(2)° γ=90.00°

4-Methyl-2,3-dihydro-1H-1,5-benzodiazepin-2-one monohydrate

C₁₀H₁₀N₂O_,H₂O

Saber, Asmaa Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 6 o1408

a=4.90130(10)Å b=7.31480(10)Å c=13.5688(2)Å

α=85.3750(10)° β=83.9590(10)° γ=83.8070(10)°

3-Benzyl-6-bromo-2-(2-furyl)-3H-imidazo[4,5-b]pyridine

C₁₇H₁₂BrN₃O

Ouzidan, Younès Rodi, Youssef Kandri Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 7 o1874

a=15.8422(3)Å b=5.47470(10)Å c=18.4243(3)Å

α=90.00° β=111.5090(10)° γ=90.00°

1,5-Dimethyl-3-propargyl-1H-1,5-benzodiazepine- 2,4(3H,5H)-dione

C₁₄H₁₄N₂O₂

Dardouri, Rachid Ouazzani Chahdi, F.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 7 o1797

a=16.0768(3)Å b=17.1087(3)Å c=8.9530(2)Å

α=90.00° β=93.7010(10)° γ=90.00°

Pyrrolo[2,1-c][1,4]benzodiazepine-5,11-dithione

C₁₂H₁₂N₂S₂

Ourahou, Sarah Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 7 o1653

a=13.9831(5)Å b=10.0134(3)Å c=8.2670(3)Å

α=90.00° β=97.0890(10)° γ=90.00°

4-Allyl-6-bromo-2-phenyl-4H-imidazo[4,5-b]pyridine monohydrate

C₁₅H₁₂BrN_3,H₂O

Ouzidan, Younès Rodi, Youssef Kandri Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 8 o1903

a=7.43630(10)Å b=9.42380(10)Å c=11.0829(2)Å

α=68.0760(10)° β=74.6370(10)° γ=79.7360(10)°

6-Bromo-1,3-dimethyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

C₈H₈BrN₃O

Dahmani, Siham Rodi, Youssef Kandri Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 8 o1904

a=21.7981(4)Å b=3.99290(10)Å c=20.6636(3)Å

α=90.00° β=95.3980(10)° γ=90.00°

N'-(1-Allyl-2-oxoindolin-3-ylidene)benzohydrazide

C₁₈H₁₅N₃O₂

Alsubari, Abdulsalam Moussaif, Ahmed Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 8 o1905

a=7.5921(2)Å b=15.1968(4)Å c=12.8716(3)Å

α=90.00° β=94.481(2)° γ=90.00°

1-Benzyl-3-methylquinoxalin-2(1H)-one

C₁₆H₁₄N₂O

Ramli, Youssef Moussaif, Ahmed Zouihri, Hafid Lazar, Saïd Essassi, E. M.

Acta Crystallographica Section E (2010) 66, 8 o1922

a=7.4433(2)Å b=17.5444(5)Å c=18.0598(7)Å

α=118.034(2)° β=100.217(2)° γ=92.7260(10)°

Ethyl 2-(2-oxo-4-phenyl-2,3-dihydro-1H-1,5-benzodiazepin-1-yl)acetate

C₁₉H₁₈N₂O₃

Ballo, Daouda Ahabchane, Noureddine Hamou Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 8 o2070

a=12.5198(4)Å b=11.7911(3)Å c=11.2058(3)Å

α=90.00° β=97.843(2)° γ=90.00°

1-[2-(2-Oxo-1,3-oxazolidin-3-yl)ethyl]-4-phenyl-1H- 1,5-benzodiazepin-2(3H)-one

C₂₀H₁₉N₃O₃

Ballo, Daouda Ahabchane, Noureddine Hamou Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 8 o2080

a=9.0163(5)Å b=11.6671(6)Å c=16.2019(8)Å

α=90.00° β=90.00° γ=90.00°

1,5-Dimethyl-3-[(3-phenyl-4,5-dihydro-1,2-oxazol-5-yl)methyl]- 1H-1,5-benzodiazepine-2,4(3H,5H)-dione

C₂₁H₂₁N₃O₃

Dardouri, Rachida Kandri Rodi, Youssef Saffon, Nathalie El Ammari, Lahcen Essassi, El Mokhtar

Acta Crystallographica Section E (2010) 66, 11 o2983

a=9.3491(2)Å b=6.97220(10)Å c=27.9201(5)Å

α=90.00° β=93.1570(10)° γ=90.00°

4-(1,3-Benzothiazol-2-yl)-5-methyl-2-phenyl-1-propynyl- 1H-pyrazol-3(2H)-one

C₂₀H₁₅N₃OS

Chakib, Imane Zerzouf, Abdelfettah Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 11 o2843

a=4.82210(10)Å b=9.3698(2)Å c=37.6990(9)Å

α=90.00° β=90.00° γ=90.00°

3-(6-Bromohexyl)-1,5-dimethyl-1H-1,5-benzodiazepine- 2,4(3H,5H)-dione

C₁₇H₂₃BrN₂O₂

Dardouri, Rchida Ouazzani Chahdi, Fouad Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 11 o2804

a=7.52140(10)Å b=9.3693(2)Å c=23.8686(5)Å

α=90.00° β=91.7500(10)° γ=90.00°

3-(12-Bromododecyl)-1,5-dimethyl-1H-1,5-benzodiazepine- 2,4(3H,5H)-dione

C₂₃H₃₅BrN₂O₂

Dardouri, Rchida Ouazzani Chahdi, Fouad Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 11 o2805

a=7.59710(10)Å b=10.5032(2)Å c=28.7129(5)Å

α=90.00° β=95.2130(10)° γ=90.00°

1-Allyl-4-(1,3-benzothiazol-2-yl)-5-methyl-2-phenyl- 1H-pyrazol-3(2H)-one

C₂₀H₁₇N₃OS

Chakib, Imane Zerzouf, Abdelfettah Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 11 o2842

a=17.8734(5)Å b=10.4297(2)Å c=18.9578(4)Å

α=90.00° β=90.00° γ=90.00°

3-[2-(1H-Benzimidazol-2-ylsulfanyl)ethyl]-1,3-oxazolidin-2-one

C₁₂H₁₃N₃O₂S

Moussaif, Ahmed Essassi, El Mokhtar Lazar, Said Zouihri, Hafid Leger, Jean Michel

Acta Crystallographica Section E (2010) 66, 12 o3137

a=8.2580(10)Å b=10.0740(10)Å c=29.201(3)Å

α=90.00° β=90.00° γ=90.00°

7-Chloro-1,5-dipropargyl-1H-1,5-benzodiazepine- 2,4(3H,5H)-dione

C₁₅H₁₁ClN₂O₂

Dardouri, Rachid Kandri Rodi, Youssef Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 12 o3228

a=10.7755(3)Å b=7.6580(2)Å c=16.7221(5)Å

α=90.00° β=103.6210(10)° γ=90.00°

1-Allyl-3-methyl-3',5'-diphenylspiro[quinoxaline- 2(1H),2'(3'H)-[1,3,4]thiadiazole]

C₂₅H₂₂N₄S

Anothane, Caleb Ahoya Bouhfid, Rachid Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2010) 66, 12 o3227

a=7.92010(10)Å b=10.07130(10)Å c=13.6642(2)Å

α=78.2960(10)° β=81.2770(10)° γ=89.8260(10)°

1,3-Diallyl-5-chloro-1H-benzimidazol-2(3H)-one

C₁₃H₁₃ClN₂O

Ouzidan, Younes Kandri Rodi, Y.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 2 o520

a=7.88310(10)Å b=15.2481(3)Å c=10.3593(2)Å

α=90.00° β=93.0560(10)° γ=90.00°

1,3,3,5-Tetramethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

C₁₃H₁₆N₂O₂

Dardouri, Rachida Rodi, Youssef Kandri Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 4 o783

a=7.51120(10)Å b=10.1731(2)Å c=15.8697(3)Å

α=90.00° β=103.6750(10)° γ=90.00°

3-Benzoyl-1,5-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-\ dione

C₁₈H₁₆N₂O₃

Dardouri, Rachida Rodi, Youssef Kandri Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 4 o849

a=7.78270(10)Å b=23.7595(4)Å c=8.6315(2)Å

α=90.00° β=105.6140(10)° γ=90.00°

5-Nitro-1-n-octyl-1H-benzimidazol-2(3H)-one

C₁₅H₂₁N₃O₃

Ouzidan, Younes Kandri Rodi, Y.Saffon, Natalie Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 3 o558

a=4.9997(3)Å b=11.4942(6)Å c=13.8739(7)Å

α=74.214(3)° β=79.637(4)° γ=84.108(4)°

1-n-decyl-5-nitro-1H-benzimidazol-2(3H)-one

C₁₇H₂₅N₃O₃

Ouzidan, Younes Kandri Rodi, Y.Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 3 o613

a=5.4933(2)Å b=10.3063(4)Å c=16.1655(6)Å

α=106.504(2)° β=98.545(2)° γ=96.809(2)°

rac-(3S,4S)-3-Hydroxy-4-phenyl-1-[(S)-(3-phenyl- 4,5-dihydro-1,2-oxazol-5-yl)methyl]-4,5-dihydro-1H-1,5-benzodiazepin- 2(3H)-one

C₂₅H₂₃N₃O₃

Rida, Mohamed Essassi, El Mokhtar Massip, Stéphane Lazar, Saïd Zouihri, Hafid

Acta Crystallographica Section E (2011) 67, 4 o945-o946

a=8.981(2)Å b=9.044(2)Å c=13.6850(10)Å

α=95.373(10)° β=102.433(10)° γ=100.03(2)°

1,3-Dibenzyl-1H-anthra[1,2-d]imidazole-2,6,11(3H)-trione

C₂₉H₂₀N₂O₃

Afrakssou, Zahra Kandri Rodi, Youssef Capet, Frédéric Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 5 o1253-o1254

a=8.1389(3)Å b=12.8748(4)Å c=21.5528(8)Å

α=90.00° β=90.00° γ=90.00°

3-[2-(6-Bromo-2-phenyl-3H-imidazo[4,5-b]pyridin- 3-yl)ethyl]-1,3-oxazolidin-2-one

C₁₇H₁₅BrN₄O₂

Ouzidan, Younes Jasinski, Jerry P.Butcher, Raymond J.Golen, James A.Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 5 o1095

a=11.3553(6)Å b=11.5915(5)Å c=12.2542(8)Å

α=90.00° β=98.685(6)° γ=90.00°

3-{2-[(3-Phenylquinoxalin-2-yl)oxy]ethyl}-1,3-oxazolidin-2-one

C₁₉H₁₇N₃O₃

Daouda, Ballo Brelot, Lydia Doumbia, Mouhamadou Lamine Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 5 o1235

a=10.1392(4)Å b=9.1398(4)Å c=34.8462(15)Å

α=90.00° β=90.00° γ=90.00°

1-allyl-3-phenylquinoxalin-2(1H)-one

C₁₇H₁₄N₂O

Benzeid, Hanane Bouhfid, Rachid Massip, Stephane Leger, Jean Michel Essassi, El Mokhtar

Acta Crystallographica Section E (2011) 67, 11 o2990

a=15.123(2)Å b=7.0390(10)Å c=26.405(3)Å

α=90.00° β=95.250(10)° γ=90.00°

1-Decyl-6-nitro-1H-benzimidazol-2(3H)-one

C₁₇H₂₅N₃O₃

Ouzidan, Younes Kandri Rodi, Youssef Essassi, El Mokhtar Luis, Santiago V.Bolte, Michael El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 11 o2937

a=32.9827(6)Å b=4.55881(9)Å c=29.3435(5)Å

α=90.00° β=109.481(2)° γ=90.00°

1,3-Bis[2-hydroxy-2-(6-methoxy-2,2-dimethyl-3a,5,6,6a-tetrahydro-2H- furo[2,3-d][1,3]dioxol-5-yl)ethyl]-2,3-dihydro-1H- 1,3-benzodiazol-2-one

C₂₇H₃₈N₂O₁₁

Lakhrissi, Brahim Massoui, Mohamed Ramli, Youssef Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2012) 68, 2 o351

a=30.5551(8)Å b=5.31320(10)Å c=17.8757(5)Å

α=90.00° β=98.267(2)° γ=90.00°

2-Hydroxy-2,3,5,10,11,11a-hexahydro-1H-pyrrolo[2,1- c][1,4]benzodiazepine-5,11-dione

C₁₂H₁₂N₂O₃

Ourahou, Sarah Zouihri, Hafid Massoui, Mohamed Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 8 o1906

a=4.8366(2)Å b=25.7449(11)Å c=8.5420(4)Å

α=90.00° β=96.509(2)° γ=90.00°

4-(Prop-2-ynyl)-2H-1,4-benzothiazin-3(4H)-one

C₁₁H₉NOS

Sebbar, Nada Kheira Zerzouf, Abdelfettah Essassi, El Mokhtar Saadi, Mohamed El Ammari, Lahcen

Acta Crystallographica Section E (2014) 70, 6 o641

a=9.005(2)Å b=10.889(3)Å c=10.341(3)Å

α=90.00° β=104.565(7)° γ=90.00°

(2Z)-2-Benzylidene-4-n-utyl-3,4-dihydro-2H-1,4-benzothiazin-3-one

C₁₉H₁₉NOS

Sebbar, Nada Kheira El Fal, Mohammed Essassi, El Mokhtar Saadi, Mohamed El Ammari, Lahcen

Acta Crystallographica Section E (2014) 70, 6 o686

a=8.7717(13)Å b=8.8631(13)Å c=12.3184(16)Å

α=88.283(9)° β=82.302(9)° γ=60.895(8)°

N'-(3-Methylquinoxalin-2-yl)-N'-phenylbenzohydrazide

C₂₂H₁₈N₄O

Ramli, Youssef Moussaif, Ahmed Zouihri, Hafid Bourichi, Houda Essassi, El Mokhtar

Acta Crystallographica Section E (2011) 67, 6 o1374

a=18.6809(12)Å b=10.5840(8)Å c=9.5860(6)Å

α=90.00° β=100.108(3)° γ=90.00°

1-Acetyl-6-bromo-1H-imidazo[4,5-b]pyridin-2(3H)-one

C₈H₆BrN₃O₂

Dahmani, Siham Kandri Rodi, Youssef Luis, Santiago V.Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 6 o1375

a=4.8302(15)Å b=9.645(3)Å c=9.809(3)Å

α=81.542(7)° β=85.735(7)° γ=89.676(8)°

Ethyl 8-amino-6-bromoimidazo[1,2-a]pyridine-2-carboxylate

C₁₀H₁₀BrN₃O₂

Dahmani, Siham Kandri Rodi, Youssef Luis, Santiago V.Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 6 o1390

a=8.366(2)Å b=11.842(3)Å c=22.743(5)Å

α=90.00° β=98.328(6)° γ=90.00°

6-Bromo-3-methyl-2-phenyl-3H-imidazo[4,5-b]pyridine

C₁₃H₁₀BrN₃

Ouzidan, Younes Essassi, El Mokhtar Luis, Santiago V.Bolte, Michael El Ammari, Lahcen

Acta Crystallographica Section E (2011) 67, 7 o1684

a=13.7138(4)Å b=6.7088(2)Å c=25.3217(7)Å

α=90.00° β=90.00° γ=90.00°

1,3-Dibenzyl-5-chloro-1H-benzimidazol-2(3H)-one

C₂₁H₁₇ClN₂O

Dardouri, Rachida Rodi, Youssef Kandri Ladeira, Sonia Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 8 o2136

a=11.0380(4)Å b=9.2863(3)Å c=33.2679(13)Å

α=90.00° β=92.297(2)° γ=90.00°

1,3-Bis[3-(1,3-dioxoisoindolin-2-yl)propyl]-1H- anthra[1,2-d]imidazole-2,6,11(3H)-trione

C₃₇H₂₆N₄O₇

Afrakssou, Zahra Rodi, Youssef Kandri Capet, Frédéric Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2011) 67, 8 o2137

a=8.4278(2)Å b=13.1258(3)Å c=13.7966(3)Å

α=94.3590(10)° β=92.4720(10)° γ=105.3510(10)°

5-(Pyridin-4-ylmethyl)-1H-pyrazolo[3,4-d]pyrimidin- 4(5H)-one

C₁₁H₉N₅O

Alsubari, Abdulsalam Ramli, Youssef Essassi, El Mokhtar Zouihri, Hafid

Acta Crystallographica Section E (2011) 67, 8 o1926

a=4.6371(3)Å b=19.2731(10)Å c=5.8593(3)Å

α=90.00° β=102.498(2)° γ=90.00°

1,1'-Dibenzyl-5,5''-dichloro-1,1'',2,2''-tetrahydrodispiro[indole-3,7'- [6,9]diazatricyclo[7.3.0.0^2,6^]dodecane-8',3''-indole]-2,2''-dione

C₃₈H₃₄Cl₂N₄O₂

Al Mamari, Khalil Ennajih, Hamid Bouhfid, Rachid Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2012) 68, 6 o1664

a=12.0421(2)Å b=16.9085(2)Å c=15.9316(2)Å

α=90.00° β=101.2430(10)° γ=90.00°

1-Phenyl-3H-2,3-benzodiazepin-4(5H)-one

C₁₅H₁₂N₂O

Daouda, Ballo Bihel, Frédéric Doumbia, Mouhamadou Lamine Essassi, El Mokhtar Ng, Seik Weng

Acta Crystallographica Section E (2012) 68, 8 o2443

a=5.47180(10)Å b=8.40200(10)Å c=26.3250(5)Å

α=90.00° β=90.00° γ=90.00°

5-Nitro-1,3-bis(prop-2-ynyl)-1H-1,3-benzimidazol-2(3H)-one

C₁₃H₉N₃O₃

Kandri Rodi, Youssef Misbahi, Khalid El-Ghayoury, Abdelkrim Zorina, Leokadiya Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2013) 69, 7 o1159

a=20.0988(16)Å b=4.2645(3)Å c=28.669(2)Å

α=90° β=90° γ=90°

1-Allyl-3-benzyl-1H-benzimidazol-2(3H)-one

C₁₇H₁₆N₂O

Kandri Rodi, Youssef Haoudi, Amal Capet, Frédéric Mazzah, Ahmed Essassi, El Mokhtar El Ammari, Lahcen

Acta Crystallographica Section E (2013) 69, 9 o1477-o1478

a=9.0667(2)Å b=9.3922(2)Å c=9.6486(2)Å

α=94.2180(10)° β=113.5430(10)° γ=106.2650(10)°